TA Instruments

AR1769-0002f

28/03/2013 10:05:55

Sample name	DI 40 mm AL P100B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1769
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 10:05:55

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	6.113	-38.423	10000	20.0	5.886	30.996	-3.058	12.23	-0.2501	9369	5.4017	62.68	10.803	1080.3	3.411E-3	0.0	0.5
1.9920	9.816	13.118	10000	20.0	5.890	31.992	1.044	19.63	0.05317	9373	13.1272	24.32	26.254	2625.4	3.411E-3	0.0	0.5
2.9960	15.47	24.934	10000	20.0	5.890	32.996	1.984	30.94	0.06414	9375	26.8248	9.796	53.650	5365.0	3.411E-3	0.0	0.5
3.9960	18.41	32.671	10000	20.0	5.893	33.996	2.600	36.83	0.07059	9378	40.7693	6.914	81.539	8153.9	3.411E-3	0.1	0.6
5.0200	24.67	51.084	10000	20.0	5.891	35.020	4.065	49.34	0.08239	9375	67.5267	3.851	135.05	13505	3.411E-3	0.1	0.6
6.0120	31.58	76.242	10000	20.0	5.887	36.012	6.067	63.17	0.09605	9370	106.6160	2.348	213.23	21323	3.411E-3	0.1	0.6
7.0120	34.03	86.192	10000	20.0	5.887	37.012	6.859	68.05	0.1008	9369	126.4020	2.023	252.80	25280	3.411E-3	0.1	0.6
8.0120	39.30	107.83	10000	20.0	5.882	38.012	8.581	78.60	0.1092	9362	165.7600	1.515	331.52	33152	3.411E-3	0.1	0.6
9.0120	46.03	140.33	10000	20.0	5.872	39.012	11.17	92.05	0.1213	9346	223.3930	1.103	446.79	44679	3.411E-3	0.2	0.7
10.020	50.95	167.36	10000	20.0	5.869	40.020	13.32	101.9	0.1307	9341	274.6140	0.8997	549.23	54923	3.411E-3	0.2	0.7
11.012	55.71	194.73	10000	20.0	5.864	41.012	15.50	111.4	0.1391	9332	325.9370	0.7516	651.87	65187	3.411E-3	0.2	0.7
11.992	60.09	222.26	10000	20.0	5.858	41.992	17.69	120.2	0.1472	9323	377.5110	0.6455	755.02	75502	3.411E-3	0.2	0.7
12.996	64.40	251.33	10000	20.0	5.853	42.996	20.00	128.8	0.1553	9315	434.9150	0.5615	869.83	86983	3.411E-3	0.2	0.7
14.012	69.14	284.55	10000	20.0	5.847	44.012	22.64	138.3	0.1638	9306	498.7980	0.4867	997.60	99760	3.411E-3	0.2	0.7
14.996	75.67	333.08	10000	20.0	5.835	44.996	26.51	151.3	0.1751	9287	593.9820	0.4055	1188.0	1.1880E5	3.411E-3	0.2	0.7
15.996	79.92	367.44	10000	20.0	5.828	45.996	29.24	159.8	0.1829	9276	664.0600	0.3631	1328.1	1.3281E5	3.411E-3	0.3	0.8
16.996	84.52	405.41	10000	20.0	5.818	46.996	32.26	169.0	0.1909	9259	740.4550	0.3240	1480.9	1.4809E5	3.411E-3	0.3	0.8
17.996	90.97	467.95	10000	20.0	5.803	47.996	37.24	181.9	0.2047	9235	855.1670	0.2790	1710.3	1.7103E5	3.411E-3	0.3	0.8
19.012	95.02	500.82	10000	20.0	5.797	49.012	39.85	190.0	0.2097	9226	930.9340	0.2555	1861.9	1.8619E5	3.411E-3	0.3	0.8
20.020	99.38	546.70	10000	20.0	5.782	50.020	43.51	198.8	0.2189	9203	1020.2000	0.2329	2040.4	2.0404E5	3.411E-3	0.3	0.8
21.012	105.8	616.58	10000	20.0	5.769	51.012	49.07	211.6	0.2318	9181	1153.0200	0.2050	2306.0	2.3060E5	3.411E-3	0.4	0.9
21.996	109.9	663.20	10000	20.0	5.748	51.996	52.78	219.8	0.2402	9149	1242.4600	0.1894	2484.9	2.4849E5	3.411E-3	0.4	0.9
22.996	114.2	709.73	10000	20.0	5.729	52.996	56.48	228.4	0.2472	9119	1343.2500	0.1747	2686.5	2.6865E5	3.411E-3	0.4	0.9
24.012	120.6	797.99	10000	20.0	5.712	54.012	63.50	241.3	0.2632	9092	1495.2600	0.1562	2990.5	2.9905E5	3.411E-3	0.4	0.9
24.996	124.7	843.56	10000	20.0	5.697	54.996	67.13	249.4	0.2691	9066	1596.5601	0.1457	3193.1	3.1931E5	3.411E-3	0.4	0.9
26.012	129.0	904.19	10000	20.0	5.685	56.012	71.95	258.1	0.2788	9048	1711.2300	0.1358	3422.5	3.4225E5	3.411E-3	0.4	0.9
27.016	135.4	996.62	10000	20.0	5.650	57.016	79.31	270.9	0.2928	8992	1881.5601	0.1226	3763.1	3.7631E5	3.411E-3	0.5	1.0
27.996	139.5	1052.4	10000	20.0	5.629	57.996	83.75	279.1	0.3001	8959	1995.4200	0.1150	3990.8	3.9908E5	3.411E-3	0.5	1.0
29.020	143.6	1115.6	10000	20.0	5.607	59.020	88.77	287.3	0.3090	8924	2115.6399	0.1081	4231.3	4.2313E5	3.411E-3	0.5	1.0
30.020	150.0	1210.9	10000	20.0	5.590	60.020	96.36	300.1	0.3211	8897	2305.4199	0.09883	4610.8	4.6108E5	3.411E-3	0.5	1.0
31.012	154.1	1280.9	10000	20.0	5.561	61.012	101.9	308.3	0.3307	8850	2431.8501	0.09313	4863.7	4.8637E5	3.411E-3	0.5	1.0
31.996	158.2	1354.1	10000	20.0	5.554	61.996	107.8	316.5	0.3405	8839	2566.3301	0.08825	5132.7	5.1327E5	3.411E-3	0.5	1.0
33.012	164.6	1451.3	10000	20.0	5.514	63.012	115.5	329.3	0.3507	8776	2773.1799	0.08094	5546.4	5.5464E5	3.411E-3	0.6	1.1
34.012	168.8	1517.4	10000	20.0	5.503	64.012	120.8	337.6	0.3577	8758	2912.2500	0.07686	5824.5	5.8245E5	3.411E-3	0.6	1.1
35.016	174.9	1632.0	10000	20.0	5.440	65.016	129.9	349.8	0.3713	8657	3127.0801	0.07077	6254.2	6.2542E5	3.411E-3	0.6	1.1
36.012	179.1	1693.2	10000	20.0	5.421	66.012	134.7	358.2	0.3761	8628	3278.7300	0.06724	6557.5	6.5575E5	3.411E-3	0.6	1.1
36.996	183.3	1782.0	10000	20.0	5.393	66.996	141.8	366.5	0.3869	8583	3432.8000	0.06389	6865.6	6.8656E5	3.411E-3	0.6	1.1
38.012	189.3	1896.4	10000	20.0	5.352	68.012	150.9	378.6	0.3986	8517	3657.5200	0.05943	7315.0	7.3150E5	3.411E-3	0.6	1.1
39.012	193.5	1976.9	10000	20.0	5.339	69.012	157.3	386.9	0.4066	8498	3823.1001	0.05677	7646.2	7.6462E5	3.411E-3	0.7	1.2
40.016	199.7	2089.3	10000	20.0	5.291	70.016	166.3	399.3	0.4164	8422	4068.0901	0.05281	8136.2	8.1362E5	3.411E-3	0.7	1.2
41.012	203.7	2163.9	10000	20.0	5.255	71.012	172.2	407.4	0.4227	8364	4232.3599	0.05040	8464.7	8.4647E5	3.411E-3	0.7	1.2
42.012	210.0	2254.6	10000	20.0	5.214	72.012	179.4	419.9	0.4273	8299	4499.4502	0.04707	8998.9	8.9989E5	3.412E-3	0.7	1.2
42.996	214.1	2396.7	10000	20.0	5.182	72.996	190.7	428.1	0.4455	8247	4674.1602	0.04499	9348.3	9.3483E5	3.412E-3	0.7	1.2
43.996	218.1	2481.8	10000	20.0	5.146	73.996	197.5	436.2	0.4527	8190	4850.7700	0.04304	9701.5	9.7015E5	3.411E-3	0.7	1.2
45.016	224.3	2613.2	10000	20.0	5.097	75.016	207.9	448.5	0.4636	8112	5128.4502	0.04033	10257	1.0257E6	3.411E-3	0.8	1.3
45.992	228.4	2701.4	10000	20.0	5.081	75.992	215.0	456.8	0.4706	8087	5317.8198	0.03876	10636	1.0636E6	3.411E-3	0.8	1.3
47.012	234.5	2845.4	10000	20.0	5.018	77.012	226.4	468.9	0.4829	7987	5602.5298	0.03632	11205	1.1205E6	3.411E-3	0.8	1.3
47.996	238.5	2931.0	10000	20.0	4.994	77.996	233.2	477.0	0.4890	7949	5797.1499	0.03494	11594	1.1594E6	3.411E-3	0.8	1.3
48.996	242.6	3024.7	10000	20.0	4.947	78.996	240.7	485.3	0.4960	7874	6000.2700	0.03343	12001	1.2001E6	3.411E-3	0.8	1.3
49.996	248.8	3178.4	10000	20.0	4.888	79.996	252.9	497.5	0.5084	7779	6304.5898	0.03142	12609	1.2609E6	3.411E-3	0.8	1.3
51.012	252.8	3277.3	10000	20.0	4.894	81.012	260.8	505.6	0.5158	7789	6509.8701	0.03047	13020	1.3020E6	3.411E-3	0.9	1.4
52.008	259.0	3424.7	10000	20.0	4.804	82.008	272.5	518.0	0.5261	7645	6831.6001	0.02849	13663	1.3663E6	3.411E-3	0.9	1.4
53.000	263.1	3530.0	10000	20.0	4.768	83.000	280.9	526.1	0.5339	7588	7045.9502	0.02741	14092	1.4092E6	3.411E-3	0.9	1.4
54.012	269.1	3680.8	10000	20.0	4.707	84.012	292.9	538.2	0.5442	7491	7374.0400	0.02586	14748	1.4748E6	3.411E-3	0.9	1.4
54.996	273.3	3777.7	10000	20.0	4.684	84.996	300.6	546.5	0.5500	7455	7605.5298	0.02496	15211	1.5211E6	3.411E-3	0.9	1.4
55.996	277.3	3888.1	10000	20.0	4.616	85.996	309.4	554.7	0.5578	7346	7827.8901	0.02388	15656	1.5656E6	3.411E-3	0.9	1.4
57.012	283.4	4030.9	10000	20.0	4.609	87.012	320.8	566.7	0.5660	7335	8168.2998	0.02284	16337	1.6337E6	3.411E-3	1.0	1.5
57.996	287.5	4133.6	10000	20.0	4.507	87.996	328.9	574.9	0.5722	7173	8411.4004	0.02170	16823	1.6823E6	3.411E-3	1.0	1.5
58.996	293.6	4335.1	10000	20.0	4.487	88.996	345.0	587.2	0.5875	7141	8767.2197	0.02071	17534	1.7534E6	3.411E-3	1.0	1.5
60.016	297.6	4493.8	10000	20.0	4.440	90.016	357.6	595.1	0.6009	7067	9006.7305	0.01995	18013	1.8013E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	300.0	4498.3	10000	20.0	4.380	90.996	358.0	600.0	0.5966	6972	315.9640	0.01937	631.93	63193	3.411E-3	0.0	1.5
2.0080	300.0	4506.7	10000	20.0	4.371	92.008	358.6	600.0	0.5977	6956	565.0220	0.01932	1130.0	1.1300E5	3.411E-3	0.0	1.5
3.0080	300.0	4509.2	10000	20.0	4.385	93.008	358.8	600.0	0.5980	6978	818.6390	0.01938	1637.3	1.6373E5	3.411E-3	0.1	1.6
3.9960	300.0	4502.0	10000	20.0	4.431	93.996	358.3	600.0	0.5971	7052	1193.2100	0.01959	2386.4	2.3864E5	3.411E-3	0.1	1.6
4.9920	300.0	4522.0	10000	20.0	4.397	94.992	359.8	600.0	0.5998	6998	1444.5100	0.01944	2889.0	2.8890E5	3.411E-3	0.1	1.6
5.9960	300.0	4489.0	10000	20.0	4.331	95.996	357.2	600.0	0.5954	6893	1822.7000	0.01915	3645.4	3.6454E5	3.411E-3	0.1	1.6
6.9920	300.0	4503.8	10000	20.0	4.382	96.992	358.4	600.0	0.5974	6974	2073.0400	0.01937	4146.1	4.1461E5	3.411E-3	0.1	1.6
7.9960	300.0	4541.1	10000	20.0	4.439	97.996	361.4	600.0	0.6023	7065	2324.2900	0.01963	4648.6	4.6486E5	3.411E-3	0.1	1.6
8.9960	300.0	4512.7	10000	20.0	4.419	98.996	359.1	600.0	0.5985	7033	2701.2700	0.01954	5402.5	5.4025E5	3.411E-3	0.1	1.6
9.9920	300.0	4514.0	10000	20.0	4.403	99.992	359.2	600.0	0.5987	7008	2952.5500	0.01947	5905.1	5.9051E5	3.411E-3	0.2	1.7
10.996	300.0	4524.8	10000	20.0	4.351	100.996	360.1	600.0	0.6002	6925	3203.9399	0.01924	6407.9	6.4079E5	3.411E-3	0.2	1.7
11.992	300.0	4533.1	10000	20.0	4.461	101.992	360.7	600.0	0.6012	7100	3580.8601	0.01972	7161.7	7.1617E5	3.411E-3	0.2	1.7
12.992	300.0	4500.5	10000	20.0	4.397	102.992	358.1	600.0	0.5969	6998	3832.1101	0.01944	7664.2	7.6642E5	3.411E-3	0.2	1.7
13.996	300.0	4557.3	10000	20.0	4.421	103.996	362.7	599.9	0.6045	7036	4209.2500	0.01955	8418.5	8.4185E5	3.411E-3	0.2	1.7
14.992	300.0	4566.1	10000	20.0	4.438	104.992	363.4	599.9	0.6056	7064	4460.5498	0.01962	8921.1	8.9211E5	3.411E-3	0.2	1.7
15.992	300.0	4505.8	10000	20.0	4.403	105.992	358.6	600.1	0.5975	7008	4711.6699	0.01946	9423.3	9.4233E5	3.411E-3	0.3	1.8
16.992	300.0	4477.8	10000	20.0	4.361	106.992	356.3	600.1	0.5938	6941	5088.7100	0.01928	10177	1.0177E6	3.411E-3	0.3	1.8
17.992	300.0	4504.8	10000	20.0	4.403	107.992	358.5	600.0	0.5974	7007	5347.2202	0.01946	10694	1.0694E6	3.411E-3	0.3	1.8
18.996	300.0	4526.8	10000	20.0	4.392	108.996	360.2	600.0	0.6003	6990	5720.7998	0.01941	11442	1.1442E6	3.411E-3	0.3	1.8
19.992	300.0	4515.5	10000	20.0	4.388	109.992	359.3	600.0	0.5988	6983	5968.4800	0.01940	11937	1.1937E6	3.411E-3	0.3	1.8
21.008	300.0	4503.7	10000	20.0	4.413	111.008	358.4	600.0	0.5973	7023	6221.8599	0.01951	12444	1.2444E6	3.411E-3	0.4	1.9
21.992	300.0	4534.9	10000	20.0	4.447	111.992	360.9	600.0	0.6015	7077	6598.1001	0.01966	13196	1.3196E6	3.411E-3	0.4	1.9
22.992	300.0	4508.6	10000	20.0	4.417	112.992	358.8	600.0	0.5979	7030	6848.3999	0.01953	13697	1.3697E6	3.411E-3	0.4	1.9
23.996	300.0	4494.0	10000	20.0	4.398	113.996	357.6	600.0	0.5960	6999	7228.4199	0.01944	14457	1.4457E6	3.411E-3	0.4	1.9
24.996	300.0	4553.4	10000	20.0	4.396	114.996	362.3	600.0	0.6039	6997	7477.7100	0.01944	14955	1.4955E6	3.411E-3	0.4	1.9
25.992	300.0	4546.3	10000	20.0	4.432	115.992	361.8	600.0	0.6030	7053	7730.3999	0.01959	15461	1.5461E6	3.411E-3	0.4	1.9
27.008	300.0	4524.2	10000	20.0	4.403	117.008	360.0	600.0	0.6000	7008	8104.8198	0.01947	16210	1.6210E6	3.411E-3	0.5	2.0
27.992	300.0	4494.1	10000	20.0	4.375	117.992	357.6	600.0	0.5960	6963	8357.7998	0.01934	16716	1.6716E6	3.411E-3	0.5	2.0
28.992	300.0	4518.0	10000	20.0	4.410	118.992	359.5	600.0	0.5992	7018	8608.9600	0.01949	17218	1.7218E6	3.411E-3	0.5	2.0
30.008	300.0	4498.9	10000	20.0	4.398	120.008	358.0	600.0	0.5967	7000	8988.6797	0.01944	17977	1.7977E6	3.411E-3	0.5	2.0
30.992	300.0	4506.5	10000	20.0	4.398	120.992	358.6	600.0	0.5977	7000	9237.7598	0.01945	18476	1.8476E6	3.411E-3	0.5	2.0
31.996	300.0	4550.5	10000	20.0	4.436	121.996	362.1	600.0	0.6035	7059	9617.7998	0.01961	19236	1.9236E6	3.411E-3	0.5	2.0
33.008	300.0	4506.3	10000	20.0	4.398	123.008	358.6	600.0	0.5976	7000	9863.9297	0.01944	19728	1.9728E6	3.411E-3	0.6	2.1
33.992	300.0	4491.4	10000	20.0	4.332	123.992	357.4	600.0	0.5957	6895	10115.500	0.01915	20231	2.0231E6	3.411E-3	0.6	2.1
34.992	300.0	4519.4	10000	20.0	4.406	124.992	359.6	600.0	0.5994	7012	10492.400	0.01948	20985	2.0985E6	3.411E-3	0.6	2.1
35.992	300.0	4517.0	10000	20.0	4.405	125.992	359.5	600.0	0.5991	7010	10743.700	0.01947	21487	2.1487E6	3.411E-3	0.6	2.1
36.992	300.0	4536.9	10000	20.0	4.390	126.992	361.0	600.0	0.6017	6987	11122.500	0.01941	22245	2.2245E6	3.411E-3	0.6	2.1
37.996	300.0	4515.4	10000	20.0	4.422	127.996	359.3	600.0	0.5989	7038	11372.000	0.01955	22744	2.2744E6	3.411E-3	0.6	2.1
38.992	300.0	4562.9	10000	20.0	4.477	128.992	363.1	600.0	0.6051	7125	11623.700	0.01979	23247	2.3247E6	3.411E-3	0.6	2.1
39.992	300.0	4504.6	10000	20.0	4.358	129.992	358.5	600.0	0.5974	6936	12000.400	0.01927	24001	2.4001E6	3.411E-3	0.7	2.2
40.996	300.0	4525.0	10000	20.0	4.389	130.996	360.1	600.0	0.6001	6986	12252.500	0.01940	24505	2.4505E6	3.411E-3	0.7	2.2
41.992	300.0	4509.4	10000	20.0	4.382	131.992	358.8	600.0	0.5980	6975	12502.900	0.01937	25006	2.5006E6	3.411E-3	0.7	2.2
42.992	300.0	4559.0	10000	20.0	4.404	132.992	362.8	599.9	0.6047	7009	12880.000	0.01948	25760	2.5760E6	3.411E-3	0.7	2.2
43.992	300.0	4514.6	10000	20.0	4.402	133.992	359.3	600.0	0.5988	7006	13131.400	0.01946	26263	2.6263E6	3.411E-3	0.7	2.2
44.988	300.0	4526.8	10000	20.0	4.419	134.988	360.2	600.0	0.6003	7032	13508.400	0.01953	27017	2.7017E6	3.411E-3	0.7	2.2
45.992	300.0	4501.3	10000	20.0	4.352	135.992	358.2	600.0	0.5970	6927	13759.500	0.01924	27519	2.7519E6	3.411E-3	0.8	2.3
47.008	300.0	4544.6	10000	20.0	4.368	137.008	361.6	600.0	0.6027	6952	14011.000	0.01931	28022	2.8022E6	3.411E-3	0.8	2.3
47.992	300.0	4499.1	10000	20.0	4.407	137.992	358.0	600.0	0.5967	7014	14387.900	0.01948	28776	2.8776E6	3.411E-3	0.8	2.3
48.988	300.0	4513.7	10000	20.0	4.384	138.988	359.2	600.0	0.5986	6978	14639.200	0.01938	29278	2.9278E6	3.411E-3	0.8	2.3
49.996	300.0	4528.4	10000	20.0	4.415	139.996	360.4	600.0	0.6006	7027	14890.500	0.01952	29781	2.9781E6	3.411E-3	0.8	2.3
50.992	300.0	4500.1	10000	20.0	4.391	140.992	358.1	600.0	0.5969	6989	15267.600	0.01942	30535	3.0535E6	3.411E-3	0.8	2.3
51.996	300.0	4466.1	10000	20.0	4.343	141.996	355.4	600.0	0.5923	6912	15521.200	0.01920	31042	3.1042E6	3.411E-3	0.9	2.4
53.000	300.0	4511.1	10000	20.0	4.418	143.000	359.0	600.0	0.5983	7031	15895.900	0.01953	31792	3.1792E6	3.411E-3	0.9	2.4
53.988	300.0	4510.8	10000	20.0	4.381	143.988	359.0	600.0	0.5983	6973	16147.300	0.01937	32295	3.2295E6	3.411E-3	0.9	2.4
54.992	300.0	4512.8	10000	20.0	4.437	144.992	359.1	600.0	0.5985	7062	16398.699	0.01961	32797	3.2797E6	3.411E-3	0.9	2.4
55.992	300.0	4542.8	10000	20.0	4.424	145.992	361.5	600.0	0.6025	7041	16776.801	0.01956	33554	3.3554E6	3.411E-3	0.9	2.4
56.992	300.0	4555.8	10000	20.0	4.440	146.992	362.5	600.0	0.6043	7066	17026.801	0.01963	34054	3.4054E6	3.411E-3	0.9	2.4
57.992	300.0	4504.7	10000	20.0	4.357	147.992	358.5	600.0	0.5974	6935	17405.000	0.01926	34810	3.4810E6	3.411E-3	1.0	2.5
58.992	300.0	4532.4	10000	20.0	4.435	148.992	360.7	600.0	0.6011	7058	17655.199	0.01961	35310	3.5310E6	3.411E-3	1.0	2.5
59.992	300.0	4490.1	10000	20.0	4.402	149.992	357.3	600.0	0.5955	7006	17906.600	0.01946	35813	3.5813E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	296.5	4426.1	10000	20.0	4.466	152.000	352.2	593.1	0.5939	7109	286.0840	0.02021	572.17	57217	3.411E-3	0.0	2.5
2.0000	292.5	4304.5	10000	20.0	4.434	153.000	342.5	585.0	0.5855	7057	524.0940	0.02062	1048.2	1.0482E5	3.411E-3	0.0	2.6
3.0120	286.4	4134.3	10000	20.0	4.513	154.012	329.0	572.8	0.5744	7183	881.1390	0.02189	1762.3	1.7623E5	3.411E-3	0.1	2.6
4.0000	282.3	4050.7	10000	20.0	4.572	155.000	322.3	564.6	0.5709	7276	1120.9301	0.02283	2241.9	2.2419E5	3.411E-3	0.1	2.6
5.0000	278.3	3916.2	10000	20.0	4.576	156.000	311.6	556.5	0.5600	7283	1345.5400	0.02352	2691.1	2.6911E5	3.411E-3	0.1	2.6
6.0000	272.2	3739.1	10000	20.0	4.662	157.000	297.5	544.3	0.5467	7420	1682.7500	0.02504	3365.5	3.3655E5	3.411E-3	0.1	2.6
7.0160	268.0	3638.5	10000	20.0	4.719	158.016	289.5	536.1	0.5401	7511	1907.9399	0.02613	3815.9	3.8159E5	3.411E-3	0.1	2.6
8.0160	262.0	3466.6	10000	20.0	4.758	159.016	275.9	524.1	0.5264	7572	2227.2600	0.02757	4454.5	4.4545E5	3.411E-3	0.1	2.7
9.0160	258.0	3348.5	10000	20.0	4.790	160.016	266.5	515.9	0.5165	7623	2440.0801	0.02864	4880.2	4.8802E5	3.411E-3	0.2	2.7
10.016	251.8	3233.6	10000	20.0	4.890	161.016	257.3	503.6	0.5110	7783	2764.8501	0.03070	5529.7	5.5297E5	3.411E-3	0.2	2.7
11.016	247.7	3125.3	10000	20.0	4.889	162.016	248.7	495.5	0.5019	7782	2961.2300	0.03170	5922.5	5.9225E5	3.411E-3	0.2	2.7
12.024	241.7	2984.7	10000	20.0	4.933	163.024	237.5	483.3	0.4914	7852	3260.1001	0.03361	6520.2	6.5202E5	3.411E-3	0.2	2.7
13.000	237.5	2897.9	10000	20.0	4.975	164.000	230.6	475.0	0.4855	7918	3460.4500	0.03509	6920.9	6.9209E5	3.411E-3	0.2	2.7
14.016	233.4	2815.7	10000	20.0	5.024	165.016	224.1	466.7	0.4801	7996	3655.2600	0.03670	7310.5	7.3105E5	3.411E-3	0.2	2.8
15.016	227.3	2673.9	10000	20.0	5.084	166.016	212.8	454.6	0.4680	8091	3935.9900	0.03915	7872.0	7.8720E5	3.411E-3	0.3	2.8
16.016	223.2	2569.9	10000	20.0	5.099	167.016	204.5	446.4	0.4581	8115	4123.5601	0.04072	8247.1	8.2471E5	3.411E-3	0.3	2.8
17.016	216.9	2452.6	10000	20.0	5.132	168.016	195.2	433.8	0.4499	8168	4398.7900	0.04340	8797.6	8.7976E5	3.411E-3	0.3	2.8
18.016	212.9	2355.5	10000	20.0	5.165	169.016	187.4	425.8	0.4402	8220	4575.6499	0.04533	9151.3	9.1513E5	3.411E-3	0.3	2.8
19.016	208.8	2280.5	10000	20.0	5.199	170.016	181.5	417.6	0.4346	8275	4749.0098	0.04746	9498.0	9.4980E5	3.411E-3	0.3	2.8
20.016	202.5	2159.8	10000	20.0	5.266	171.016	171.9	405.1	0.4243	8381	5008.4199	0.05108	10017	1.0017E6	3.411E-3	0.3	2.9
21.016	198.5	2073.1	10000	20.0	5.287	172.016	165.0	397.0	0.4155	8415	5170.7998	0.05338	10342	1.0342E6	3.411E-3	0.4	2.9
22.016	192.3	1944.0	10000	20.0	5.324	173.016	154.7	384.7	0.4021	8474	5412.7900	0.05726	10826	1.0826E6	3.411E-3	0.4	2.9
23.012	188.1	1855.1	10000	20.0	5.341	174.012	147.6	376.2	0.3924	8501	5575.2598	0.06006	11151	1.1151E6	3.411E-3	0.4	2.9
24.016	184.0	1793.1	10000	20.0	5.380	175.016	142.7	368.0	0.3877	8562	5725.4102	0.06322	11451	1.1451E6	3.411E-3	0.4	2.9
25.016	177.9	1674.9	10000	20.0	5.428	176.016	133.3	355.7	0.3747	8639	5949.6201	0.06827	11899	1.1899E6	3.411E-3	0.4	2.9
26.000	173.7	1604.6	10000	20.0	5.464	177.000	127.7	347.3	0.3676	8696	6100.5698	0.07209	12201	1.2201E6	3.411E-3	0.4	3.0
27.016	167.6	1497.8	10000	20.0	5.474	178.016	119.2	335.2	0.3556	8713	6305.7500	0.07756	12612	1.2612E6	3.411E-3	0.5	3.0
28.000	163.4	1447.7	10000	20.0	5.489	179.000	115.2	326.9	0.3524	8736	6443.8198	0.08175	12888	1.2888E6	3.411E-3	0.5	3.0
29.016	159.2	1358.6	10000	20.0	5.514	180.016	108.1	318.5	0.3395	8775	6580.5898	0.08651	13161	1.3161E6	3.411E-3	0.5	3.0
30.004	153.0	1249.8	10000	20.0	5.546	181.004	99.46	306.0	0.3250	8827	6774.1602	0.09426	13548	1.3548E6	3.411E-3	0.5	3.0
31.016	148.9	1189.5	10000	20.0	5.572	182.016	94.66	297.8	0.3178	8867	6898.9902	0.09996	13798	1.3798E6	3.411E-3	0.5	3.0
32.000	144.7	1128.0	10000	20.0	5.604	183.000	89.77	289.4	0.3102	8919	7024.3901	0.1065	14049	1.4049E6	3.411E-3	0.5	3.1
33.016	138.5	1027.5	10000	20.0	5.620	184.016	81.76	277.0	0.2952	8944	7201.0098	0.1166	14402	1.4402E6	3.411E-3	0.6	3.1
34.000	134.4	972.51	10000	20.0	5.649	185.000	77.39	268.8	0.2879	8990	7310.8701	0.1244	14622	1.4622E6	3.411E-3	0.6	3.1
35.016	128.1	873.06	10000	20.0	5.657	186.016	69.48	256.1	0.2713	9004	7479.1699	0.1372	14958	1.4958E6	3.411E-3	0.6	3.1
36.016	123.8	817.26	10000	20.0	5.689	187.016	65.04	247.6	0.2627	9054	7588.7598	0.1477	15178	1.5178E6	3.411E-3	0.6	3.1
37.000	119.7	765.53	10000	20.0	5.697	188.000	60.92	239.4	0.2544	9067	7684.8999	0.1581	15370	1.5370E6	3.411E-3	0.6	3.1
38.016	113.4	683.76	10000	20.0	5.720	189.016	54.41	226.7	0.2400	9103	7834.8501	0.1771	15670	1.5670E6	3.411E-3	0.6	3.2
39.012	109.1	643.67	10000	20.0	5.732	190.012	51.22	218.1	0.2348	9123	7929.8999	0.1918	15860	1.5860E6	3.411E-3	0.7	3.2
40.000	105.0	599.78	10000	20.0	5.750	191.000	47.73	210.0	0.2272	9151	8015.0298	0.2074	16030	1.6030E6	3.411E-3	0.7	3.2
41.004	98.67	523.75	10000	20.0	5.771	192.004	41.68	197.3	0.2112	9185	8145.6299	0.2358	16291	1.6291E6	3.411E-3	0.7	3.2
42.020	94.21	477.44	10000	20.0	5.780	193.020	37.99	188.4	0.2016	9200	8233.1602	0.2591	16466	1.6466E6	3.411E-3	0.7	3.2
43.016	90.04	442.15	10000	20.0	5.792	194.016	35.19	180.1	0.1954	9218	8307.2803	0.2843	16615	1.6615E6	3.411E-3	0.7	3.2
44.000	83.66	387.77	10000	20.0	5.807	195.000	30.86	167.3	0.1844	9242	8419.0801	0.3301	16838	1.6838E6	3.411E-3	0.7	3.3
45.012	79.12	352.62	10000	20.0	5.812	196.012	28.06	158.2	0.1773	9250	8493.4297	0.3694	16987	1.6987E6	3.411E-3	0.8	3.3
46.016	74.94	319.41	10000	20.0	5.822	197.016	25.42	149.9	0.1696	9266	8555.5000	0.4125	17111	1.7111E6	3.411E-3	0.8	3.3
47.016	68.52	266.97	10000	20.0	5.833	198.016	21.24	137.0	0.1550	9283	8648.4004	0.4942	17297	1.7297E6	3.411E-3	0.8	3.3
48.016	63.90	244.39	10000	20.0	5.839	199.016	19.45	127.8	0.1522	9292	8710.1396	0.5689	17420	1.7420E6	3.411E-3	0.8	3.3
49.016	59.69	211.02	10000	20.0	5.846	200.016	16.79	119.4	0.1407	9304	8760.0996	0.6528	17520	1.7520E6	3.411E-3	0.8	3.3
50.016	55.43	187.25	10000	20.0	5.852	201.016	14.90	110.9	0.1344	9314	8809.0898	0.7577	17618	1.7618E6	3.411E-3	0.8	3.4
51.016	50.84	160.91	10000	20.0	5.857	202.016	12.80	101.7	0.1259	9322	8858.2305	0.9015	17716	1.7716E6	3.411E-3	0.9	3.4
52.016	44.12	125.61	10000	20.0	5.864	203.016	9.996	88.24	0.1133	9333	8919.6504	1.199	17839	1.7839E6	3.411E-3	0.9	3.4
52.996	39.78	104.47	10000	20.0	5.868	203.996	8.313	79.56	0.1045	9339	8956.6299	1.475	17913	1.7913E6	3.411E-3	0.9	3.4
54.012	34.92	83.479	10000	20.0	5.874	205.012	6.643	69.84	0.09512	9350	8993.0000	1.917	17986	1.7986E6	3.411E-3	0.9	3.4
55.012	29.83	63.362	10000	20.0	5.877	206.012	5.042	59.66	0.08452	9354	9023.4805	2.628	18047	1.8047E6	3.411E-3	0.9	3.4
56.000	25.47	48.622	10000	20.0	5.880	207.000	3.869	50.95	0.07595	9359	9047.3701	3.606	18095	1.8095E6	3.411E-3	0.9	3.5
57.000	20.30	32.739	10000	20.0	5.881	208.000	2.605	40.59	0.06418	9361	9071.1396	5.681	18142	1.8142E6	3.411E-3	1.0	3.5
58.000	14.54	18.566	10000	20.0	5.884	209.000	1.477	29.07	0.05082	9365	9088.4404	11.08	18177	1.8177E6	3.411E-3	1.0	3.5
59.012	9.829	8.9951	10000	20.0	5.884	210.012	0.7158	19.66	0.03641	9365	9099.7100	24.23	18199	1.8199E6	3.411E-3	1.0	3.5
60.016	6.576	3.8165	10000	20.0	5.885	211.016	0.3037	13.15	0.02309	9366	9104.6504	54.15	18209	1.8209E6	3.411E-3	1.0	3.5

